Data collection and refinement statistics.
| WRN ADP | |
|---|---|
| Space group | P 21 21 21 |
| Cell dimensions a, b, c (Å) | 54.6, 90.6, 138.2 |
| Angles α, β, γ (°) | 90, 90, 90 |
| Wavelength (Å) | 1.08 |
| Resolution (Å) | 76.0–2.20 (2.26–2.20) |
| Rmerge | 0.13 (2.3) |
| Rp.i.m. | 0.06 (1.13) |
| I/σI | 5.3 (1.0) |
| CC1/2 | 0.99 (0.50) |
| Completeness (%) | 98.8 (96.0) |
| Multiplicity | 5.5 (5.5) |
| No. of unique reflections | 35,356 (2,943) |
| Refinement statistics | |
| Resolution | 76.0–2.20 |
| Rwork/Rfree (%) | 19.6/23.5 |
| No. of atoms | |
| Protein | 4,302 |
| Solvent | 195 |
| Ligand/ion | 29 |
| Average B factors (Å2) | |
| Protein | 71.8 |
| Solvent | 68.8 |
| Ligand/ion | 76 |
| Wilson B | 48 |
| RMSD | |
| Bond lengths (Å) | 0.002 |
| Bond angles (°) | 0.534 |
| Ramachandran plot | |
| Favoured (%) | 97.3 |
| Allowed (%) | 2.7 |